Influence of sintering temperature on the microstructural and mechanical properties of cordierite synthesized from andalusite and talc

A. Benhammou; Y. El Hafiane; A. Abourriche; Y. Abouliatim; L. Nibou; A. Yaacoubi; Nicolas Tessier-Doyen; Agnès Smith; B. Tanouti

Influence of sintering temperature on the microstructural and mechanical properties of cordierite synthesized from andalusite and talc

A. Benhammou ¹ Y. El Hafiane ² A. Abourriche ² Y. Abouliatim ² L. Nibou ² A. Yaacoubi ³ Nicolas Tessier-Doyen ⁴ Agnès Smith ⁴ B. Tanouti ⁵

1 LMPEQ - Laboratoire Matériaux Procédés Environnement Qualité

2 ENSA - Ecole Nationale des Sciences Appliquées [Safi]

3 FSSM - Faculté des Sciences SEMLALIA

4 SPCTS - Science des Procédés Céramiques et de Traitements de Surface

5 Laboratoire de Chimie du Solide Mineral

Abstract : Cordierite-based ceramic has been synthesized by solid state process from andalusite and talc mixture sintered at 1300 and 1350 °C for 2 h. The phase, microstructural and thermal characterizations of the samples were investigated using X-ray diffraction (XRD), scanning electron microscope (SEM), dilatometric and thermal analysis (TG/DTA). Brazilian and three-point bending tests were performed to evaluate the mechanical properties. XRD results showed a significant improvement in the cordierite formation at 1350 °C, whereas the sintering at 1300 °C was insufficient. The SEM observation showed that the sample sintered at 1350 °C was relatively dense. As a result of this densification, the flexural and tensile strengths at 1300 °C (15.4±1.2 and 12.2±1.9 MPa, respectively) were significantly enhanced with increasing temperature to 1350 °C (32±4.2 and 18.3±3.6 MPa, respectively).

Keywords : Cordierite Talc Andalusite Sintering Mechanical properties

Type de document :

Article dans une revue

Domaine :

Chimie / Matériaux

Sciences de l'ingénieur [physics] / Matériaux

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https://hal-unilim.archives-ouvertes.fr/hal-01875322
Contributeur : Beatrice Derory <>
Soumis le : lundi 17 septembre 2018 - 11:15:00
Dernière modification le : vendredi 9 août 2019 - 15:18:07

Influence of sintering temperature on the microstructural and mechanical properties of cordierite synthesized from andalusite and talc

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Influence of sintering temperature on the microstructural and mechanical properties of cordierite synthesized from andalusite and talc

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